Standardized Calibration Procedures for Rotorless Rheometers

No rotor reheometer

1. Calibration Parameters Specification

Parameter CategoryCalibration MethodTolerance RangeReference Equipment
Temperature SystemMulti-point verification with standard thermocouples±1°C (steady-state)Class II platinum resistance thermometer
Fluctuation ≤0.5°C/30minInfrared thermal imager
Torque SystemLever-type standard torque generatorError ≤0.5% FSTorque calibration device
Clamping Force SystemStrain-gauge pressure sensor calibrationLinearity deviation ±0.5kNDigital pressure calibrator

2. Step-by-Step Calibration Workflow

2.1 Temperature System

  • Thermal Equilibrium: Stabilize at 180°C±2°C for 30min (fluctuation ≤0.3°C)
  • Spatial Uniformity: 9-point test matrix (3 layers × 3 points) recording max-min difference
  • System Adjustment: Compensate deviations via PID tuning

2.2 Torque System

  • Zeroing Procedure: Auto-zero at 23±5°C (ambient)
  • Range Verification: Apply 20%/50%/100% full-scale torque for linearity test

2.3 Clamping Force System

  • Static Calibration: Step-loading from 5-20kN
  • Dynamic Test: 10 consecutive cycles for repeatability verification

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